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Volume 2 No. 3
10 July 2013

Feng JIANG,Zhijian PENG,Yanxu ZANG,Xiuli FU

2013, 2(3): 201-212.   doi:10.1007/s40145-013-0071-z
Abstract ( 145 HTML ( 13   PDF(331KB) ( 329 )   Save

Rare-earth (RE) doping can greatly enhance the voltage gradient of ZnO-based varistors, and their nonlinear coefficient, leakage current, energy absorption capability, through-current capability and residual voltage can also be improved to certain extent. In this review, the progress on RE-doped ZnO-based varistor materials in recent years was summarized. The mechanism of RE doping on the electrical performance of ZnO varistors was analyzed. The issues in exploring new ZnO-based varistor mate...

Mahmoud Aly HAMAD

2013, 2(3): 213-217.   doi:10.1007/s40145-013-0062-0
Abstract ( 204 HTML ( 5   PDF(284KB) ( 243 )   Save

The magnetocaloric effect (MCE) achieved for La0.7Sr0.3MnO3/Ta2O5 composites has been investigated. The maximum value of magnetic entropy change of La0.7Sr0.3MnO3 composites is found to decrease slightly with the further increasing of Ta2O5 concentration. It is shown that La0.7Sr0.3MnO3/Ta2O5 composites exhibit much more uniform m...

Pavel CTIBOR,Vaclav STENGL,Zdenek PALA

2013, 2(3): 218-226.   doi:10.1007/s40145-013-0063-z
Abstract ( 247 HTML ( 5   PDF(3103KB) ( 436 )   Save

Titanium dioxide (TiO2) was elaborated by four different thermal spray techniques—(i) plasma spraying using a water-stabilized torch, (ii) plasma spraying using a gas-stabilized torch, (iii) high velocity oxy–fuel gun, and (iv) oxy–acetylene flame. The porosity of the coatings was studied by optical microscopy, nano-structural features by scanning electron microscopy (SEM), phase composition by X-ray diffraction (XRD); the microhardness, surface roughness and wear resistance were e...

Lijie QU,Muqin LI,Miao LIU,Erlin ZHANG,Chen MA

2013, 2(3): 227-234.   doi:10.1007/s40145-013-0064-y
Abstract ( 271 HTML ( 5   PDF(3237KB) ( 649 )   Save

The ultrasonic micro-arc oxidation (UMAO) was used to fabricate ceramic coatings on magnesium alloy. UMAO coatings were produced at 60 W input ultrasonic. The effects of the ultrasound on the microstructure, phase composition, elemental distribution and corrosion resistance of the coatings were extensively investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), energy-dispersive X-ray spectrometry (EDX) and electrochemical workstation. The results showed that ultrasound i...

Samita PATTANAYAK,Ashwasa PRIYADARSHAN,Ritesh SUBUDHI,Ranjan Kumar NAYAK,Rajib PADHEE

2013, 2(3): 235-241.   doi:10.1007/s40145-013-0065-x
Abstract ( 241 HTML ( 8   PDF(1792KB) ( 573 )   Save

The polycrystalline samples of Bi1-xPrxFeO3 (x = 0 and 0.1) were prepared by a solid-state reaction technique. Preliminary X-ray structural analysis has confirmed the formation of a single-phase compound. Studies of dielectric and impedance spectroscopy of the materials, carried out in wide frequency (1 kHz–1 MHz) and temperature (25–400 ℃) ranges, have provided many interesting results including significant decrement in tangent los...

Jiayan LI,Panpan CAO,Yi TAN,Lei ZHANG

2013, 2(3): 242-245.   doi:10.1007/s40145-013-0066-9
Abstract ( 345 HTML ( 8   PDF(2021KB) ( 633 )   Save

Polycarbosilane (PCS) has been widely used to fabricate silicon carbide (SiC) fibers via pyrolysis. In this paper, for improving the morphology of SiC fibers, tetraethyl orthosilicate (TEOS, m = 1 g, 3 g and 5 g, respectively) was added into the PCS precursor solution (containing 1.5 g PCS). The continuous fibers have been prepared by electrospinning, and then the SiC fibers were synthesized by calcination at 1300 ℃, 1400 ℃ and 1600 ℃ for 4 h respectively with a he...

R. V. BARDE,S. A. WAGHULEY

2013, 2(3): 246-251.   doi:10.1007/s40145-013-0067-8
Abstract ( 199 HTML ( 5   PDF(389KB) ( 239 )   Save

We investigate the DC transport properties of 60V2O5–5P2O5–(35-x)B2O3xDy2O3 (x = 0.4, 0.6, 0.8, 1.0 and 1.2 mol%) glasses as function of temperature which were prepared using the conventional melt-quenching method. These glasses are characterised by thermo gravimetric-differential thermal analysis (TG-DTA). Activation energy (EDC) is obtained from Arrhenius plots of ...

Qiming HANG,Wenke ZHOU,Xinhua ZHU,Jianmin ZHU,Zhiguo LIU,Talaat AL-KASSAB

2013, 2(3): 252-259.   doi:10.1007/s40145-013-0068-7
Abstract ( 497 HTML ( 6   PDF(6048KB) ( 307 )   Save

0.67BiFeO3–0.33BaTiO3 multiferroic ceramics doped with x mol% MnO2 (x = 2–10) were synthesized by solid-state reaction. The formation of a perovskite phase with rhombohedral symmetry was confirmed by X-ray diffraction (XRD). The average grain sizes were reduced from 0.80 μm to 0.50 μm as increasing the Mn-doped levels. Single crystalline nature of the grains was revealed by high-resolution transmission electron microscopy (HR...

K. SOWRI BABU,A. RAMACHANDRA REDDY,Ch. SUJATHA,K. VENUGOPAL REDDY,A. N. MALLIKA

2013, 2(3): 260-265.   doi:10.1007/s40145-013-0069-6
Abstract ( 337 HTML ( 10   PDF(1243KB) ( 290 )   Save

In this paper, a simple and cheap method to prepare porous ZnO by using zinc nitrate, ethanol and triethanolamine (TEA) is reported. The as-prepared sample consisted of nano and micro pores. The sample was calcined at 300 ℃, 400 ℃ and 500 ℃ with different heating rates. At 500 ℃, the nano pores disappeared but the sample maintained its micro porosity. Field emission scanning electron microscopy (FE-SEM) pictures confirmed that the size and growth of ZnO nanoparticl...

Lianfeng DUAN,Fenghui GAO,Limin WANG,Songzhe JIN,Hua WU

2013, 2(3): 266-273.   doi:10.1007/s40145-013-0070-0
Abstract ( 407 HTML ( 2   PDF(4077KB) ( 781 )   Save

MnCo2O4 octahedral structure with edge length about 500 nm was successfully synthesized by a simple hydrothermal route. With the use of NaOH, the chemical potential and the rate of ionic motion in the precursor solution were controlled, and the particle size was limited. The magnetization measurements revealed that the products exhibited ferrimagnetic characteristics with different saturation magnetization and coercivity at different measuring temperatures. In addition, ...

Lukasz WITEK,James SMAY,Nelson R. F. A. SILVA,Teja GUDA,Joo L. ONG,Paulo G. COELHO

2013, 2(3): 274-284.   doi:10.1007/s40145-013-0072-y
Abstract ( 237 HTML ( 6   PDF(1707KB) ( 281 )   Save

The objective of this study was to characterize the chemical and physical properties of bioactive ceramics prepared from an aqueous paste containing hydroxyapatite (HA) and beta tri-calcium phosphate (β-TCP). Prior to formulating the paste, HA and β-TCP were calcined at 800 ℃ and 975 ℃ (11 h), milled, and blended into 15%/85% HA/β-TCP volume-mixed paste. Fabricated cylindrical rods were subsequently sintered to 900 ℃, 1100 ℃ or 1250 ℃. T...

Jong Hyun KIM,Jung Rag YOON

2013, 2(3): 285-290.   doi:10.1007/s40145-013-0073-x
Abstract ( 257 HTML ( 6   PDF(1503KB) ( 298 )   Save

The electrical characteristics of hybrid super capacitor were evaluated by synthesizing LTO (Li4Ti5O12) using TiO2 having a hydrogen titanate nanowire form. Preparation of the hydrogen titanate nanowire was implemented by using TiO2 having size of 60 nm and NaOH, and performing synthesis at 70 ℃ for 6 h with a sonochemical method. LTO compound was synthesized at 150 ℃ for 36 h and at 180 ℃ for 36 h respectively by usi...

Subhanarayan SAHOO,Umasankar DASH,S. K. S. PARASHAR,S. M. ALI

2013, 2(3): 291-300.   doi:10.1007/s40145-013-0075-8
Abstract ( 407 HTML ( 6   PDF(1011KB) ( 333 )   Save

Nanocrystalline calcium titanate (CT) ceramic has been synthesized by a combination of solid-state reaction and high-energy ball milling. This nano-ceramic is characterized by X-ray diffraction (XRD), dielectric study and impedance spectroscopy. The XRD pattern shows single phase ceramic of orthorhombic symmetry. The frequency-dependent dielectric study shows that the dielectric constant is maximized at low frequencies and decreases with an increase in frequency. Impedance spectroscopy analys...