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Volume 5 No. 4
20 December 2016

Li ZHANG,Jie ZHANG,Zhenxing YUE,Longtu LI

2016, 5(4): 269-276.   doi:10.1007/s40145-016-0199-8
Abstract ( 275 HTML ( 3   PDF(7406KB) ( 85 )   Save

Polymer–ceramic composites were prepared by twin screw melt extrusion with high-density polyethylene (HDPE) as the matrix and polystyrene-coated BaO–Nd2O3–TiO2 (BNT) ceramics as the filling material. Interestingly, the incorporation of polystyrene (PS) by the coating route could significantly improve the thermal behaviors of the composites (HDPE–PS/BNT), besides the temperature stability of dielectric properties and thermal displacement. The microwave dielectr...

Rui GUO,Jianquan QI,Jiali LUO,Xiaoyu DONG,Longtu LI

2016, 5(4): 277-283.   doi:10.1007/s40145-016-0200-6
Abstract ( 276 HTML ( 1   PDF(3836KB) ( 296 )   Save

The sintering temperature decreases theoretically with the grain size of the ceramic powders, but it is not always right for fine grain sized nanopowders due to the inevitable agglomerations, and thus pores are hard to eliminate thoroughly during sintering. To overcome this difficulty, a new approach is designed to sintering ceramics at low temperature from nanoparticles. In this scheme, excessive dopants, such as ZnO, are synthesized into the nanoparticles, and they would be liberated again ...

Xia KONG,Yawei HU,Xiaofang WANG,Wei PAN

2016, 5(4): 284-290.   doi:10.1007/s40145-016-0201-5
Abstract ( 193 HTML ( 0   PDF(6594KB) ( 234 )   Save

A hierarchical structural surface of TiO2 film with reversibly light-switchable wettability between superhydrophobicity and superhydrophilicity on metal substrate was fabricated through simply dip-coating method from TiO2 precursor solution containing TiO2 nanoparticles with the average diameter 25 nm (P25), followed by heat-treatment and modification with fluoroalkylsilane (FAS) molecules. The morphology, phase and crystallographic structure, and chemical com...

Yongqiang CHEN,Bingbing FAN,Gang SHAO,Rui ZHANG

2016, 5(4): 291-297.   doi:10.1007/s40145-016-0202-4
Abstract ( 236 HTML ( 0   PDF(5295KB) ( 292 )   Save

Ultra-large zirconia toughened alumina (ZTA, mass ratio of Al2O3 and ZrO2 is 78:22) ceramics with eccentric circle shape were successfully sintered by microwave sintering with a multi-mode cavity at 2.45 GHz. The dimension of ZTA ceramics (green body) is 165 mm (outer diameter) × 25 mm (thickness). The optimized sintering temperature of microwave sintering is about 1500 ℃ for 30 min, and the total sintering time is about 4 h which is much shorter than t...

Hongfang SHEN,Youjun LU,Yanmin WANG,Zhidong PAN,Guozhong CAO,Xianghui YAN,Guoli FANG

2016, 5(4): 298-307.   doi:10.1007/s40145-016-0203-3
Abstract ( 363 HTML ( 0   PDF(5056KB) ( 274 )   Save

SrTiO3 nanoparticle (NP) photocatalyst was synthesized with a facile and environmental-friendly hydrothermal method using tetrabutyltitanate, strontium oxide, and ethanolamine as precursors at low temperature without alkali as mineralizer for the first time. The SrTiO3 nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), and N2 Brunauer–Emmett–Teller (BET) meth...

Bharathi PONRAJ,Rajasekhar BHIMIREDDI,K. B. R. VARMA

2016, 5(4): 308-320.   doi:10.1007/s40145-016-0204-2
Abstract ( 394 HTML ( 0   PDF(5222KB) ( 273 )   Save

Polymer nanocrystal composites were fabricated by embedding polyvinylidene fluoride (PVDF) with K0.5Na0.5NbO3 (KNN) nanocrystallites of different volume fraction using the hot-pressing technique. For comparison, PVDF–KNN microcrystal composites of the same compositions were also fabricated which facilitated the studies of the crystallite size (wide range) effect on the dielectric and piezoelectric properties. The structural, morphological, dielectric, and piez...

Jiaxin WEN,Zhipeng XIE,Wenbin CAO,Xianfeng YANG

2016, 5(4): 321-328.   doi:10.1007/s40145-016-0205-1
Abstract ( 291 HTML ( 0   PDF(3071KB) ( 416 )   Save

In this work, various backbone binders were used in wax-based binder system to formulate zirconia parts by ceramic injection molding (CIM). The effect of different backbone binders on the molding, debinding, and sintering behaviors was investigated. After blending process, the feedstock using multi-polymer components exhibited more homogeneous structure compared with that using the mono-polymer ones due to the synergistic effect of multi-polymers. During solvent debinding, some defects such a...

Xiang SUN,Hong ZHANG,Ya LIU,Jia GUO,Zhicheng LI

2016, 5(4): 329-336.   doi:10.1007/s40145-016-0206-0
Abstract ( 260 HTML ( 0   PDF(1707KB) ( 554 )   Save

Y2O3-doped Zn1-xNixO (x = 0, 0.3, 0.4, 0.5, 0.6, 0.7, and 0.9) powders were prepared by a wet chemical synthesis method, and the related ceramics were obtained by the traditional ceramic sintering technology. The phases and related electrical properties of the ceramics were investigated. The analysis of X-ray diffraction (XRD) indicates that the prepared ceramics with Ni substitution have a cubic crystalline structure. The resis...

Chunlong GUAN,Nana SUN

2016, 5(4): 337-343.   doi:10.1007/s40145-016-0207-z
Abstract ( 266 HTML ( 0   PDF(8052KB) ( 43 )   Save

A novel simple method is presented to synthesize high-purity Ti2SC powder using Ti/C/S and Ti/C/TiS2 systems by microwave hybrid heating at different temperatures in argon atmosphere. It was confirmed that the synthesis temperature is strongly dependent on the starting composition. For Ti/C/S system, Ti2SC with small amounts of TiS and TiC was synthesized at 1200 ℃. For Ti/C/TiS2 system, high-purity Ti2SC was synthesized at 800 &#x...

Manisha UPASANI

2016, 5(4): 344-355.   doi:10.1007/s40145-016-0208-y
Abstract ( 408 HTML ( 0   PDF(4443KB) ( 363 )   Save

This paper reports the comparative investigations of the structural and spectral properties of Y3Al5O12:Eu3+ (YAG:Eu) and Y3Al5O12:Eu3+,Si4+ (YAG:Eu,Si) phosphors synthesized by combustion method at low temperature. A pure phase was identified for the YAG:Eu phosphor with a suitable amount of SiO2. Rietveld refinement and analytical calculation of different structural parameters were ...